Hi all,
I am currently designing a flash distillation to separate a mixture of methanol and biodiesel. One of the standard methods for doing this to use vacuum distillation, but I am not sure how to go about finding the optimum combination of temperature/pressure. As I reduce the pressure to absolute vacuum, I don't need as much heat to achieve the separation. My vessel is small so wall thickness/vacuum vessel construction is not a problem. I plan to generate the vacuum by condensing the methanol rather than using a compressor, so I don't have to worry about compressor duty, and the condenser duty does not really change much with temperature/pressure.
What is stopping me going to full vacuum?
Any tips on the cost/benefit of vacuum systems would be appreciated.
Cheers.