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How To Remove Dissolved Oxygen In A Organic Solvents In A Reactor


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#1 sateeshkumar830

sateeshkumar830

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Posted 21 October 2016 - 08:08 PM

Dear sir,
How to remove dissolved oxygen in a organic solvents in a reactor ?
Solvents - Tetrahydrofuran 160 litres And Di iso propyl ethyl amine 900 litres, and one solid.
Reactor capacity - 3.6 Kl
We are giving nitrogen purging to that organic mixture with a flow rate of 20 LPH. How can i ensure that dissolved oxygen is removed. How to calculate the nitrogen dispersion.

#2 Bobby Strain

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Posted 21 October 2016 - 10:06 PM

Best to remove oxygen before it is placed into the reactor. Where you can control the contact with an inert stripping medium. Or vacuum.

 

Bobby



#3 sateeshkumar830

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Posted 22 October 2016 - 06:06 AM

How to remove oxygen before charging in the reactor sir?? Any simple process ??

#4 sateeshkumar830

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Posted 24 October 2016 - 04:37 AM

Best to remove oxygen before it is placed into the reactor. Where you can control the contact with an inert stripping medium. Or vacuum.


Bobby

Thank you... Suggest me any Simple process and calculation to know how much time with how much nitrogen pressure to maintain bubbling in the reactor?




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