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Chemical and Process Engineering Resources

Packed Column Design

Nov 08 2010 01:20 PM | Chris Haslego in Separation Technology ***** Share this topic:
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Designing a randomly packed column is a subtle blend of art and science. Packed columns are most frequently used to remove contaminants from a gas stream (absorption). However, packed columns can also be used to remove volatile components from a liquid stream by contacting it with an inert gas (stripping). They are also used in distillation applications where the separation is particularly difficult due to close boiling components. While we'll discuss all of these applications, we'll focus on absorption. However, the design methods are similar for any of the scenarios.

The first step in designing a packed tower is more science than art.

The equilibrium data between the contaminant and the solvent (or the distillation components) is needed for the analysis. If tabulated data for your system is unavailable and the total amount of the contaminant is small (as it usually will be), Raoult's Law can be used to estimate the equilibrium data for absorption or stripping applications. For distillation, equilibrium data can be predicted by selecting the appropriate thermodynamic model. The operating line for the tower is constructed differently depending on whether you're dealing with distillation or absorption/stripping.

packcol4
Figure 1: General Packed
Column Arrangement

Since we're focusing on absorption, we'll use it as an example. In absorption/stripping, the operating line is constructed differently depending on whether the contaminated stream can be considered "dilute" or if it must be treated as a concentrated stream. Usually, it is safe to treat the stream as dilute if the contaminant makes up less than 10 mole percent of the stream. For streams that cannot be considered dilute, the mass transfer coefficients must be evaluated in terms of the gas and liquid flows. Then, graphical evaluation of several integral relationships must be completed. This type of evaluation is outside the scope of this article and a text should be consulted for solving these types of problems. For this article, we will consider dilute streams which are more common for packed tower absorption and stripping.

Dilute streams allow the column designer to assume constant mass transfer and the operating line can be constructed in terms of the simplified balance shown below:

L out x out + G out y out = L in x in + G in y inEq. (1)

Quick Example

Suppose you wish to remove acetone from a gas stream of 10,000 mol/h in a packed column. The inlet gas contains 2.6 mole percent acetone and the outlet gas stream can contain no more than 0.5 mole percent acetone. Assume a pure water stream enters the packed tower at a rate of 8,000 mol/h.

packcol5
Figure 2: Example Packed Column

L out x out + G out y out = L in x in + G in y in
(8000) x out + (10000)(0.005) = (8000)(0)+(10000)(0.026)

x out = 0.02625

The equilibrium and operating lines are constructed as follows:

Just as in the McCabe-Thiele analysis of distillation, the equilibrium stages are stepped off between the two lines. Note that for stripping, the operating line would be on the other side of the equilibrium line.

Once the theoretical number of stages have been determined, you can proceed with the design of the column by following the three steps that we'll outline below.

packcol6
Figure 3: Constructing the Operating and Equilibrium Lines





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3 Comments

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Mahendar Errala
May 27 2013 05:04 AM

Can I get a similar example for distillation in packed column.

Thanks in advance.

 

Mahendar

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GURU KAJENDHIRAN
Jul 23 2013 06:40 AM

HAI , ANY BODY EXPLANIED ME FOR CRYOGENCIC PROCESS.

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dreambigger777
Nov 13 2013 10:30 PM

Very well explained :)