12 replies to this topic

[Quimarah]

Hello everyone!

 

I have to calculate the nitrogen required for a tank of GLYCEROL.

 

Glycerol will be stored at 50°C.

Nitrogen gas will prevent air, humidity and other contaminants from entering the tank.
A vertical atmospheric vessel designed according to API 650 standard will be used.

The tank must have external insulation with internal steam coils or coils for the circulation of low pressure steam or hot water.
Construction material: AISI 304 stainless steel.
Storage temperature: 50°C.

 

The mass flow of glycerol in the process its aproximate 10029,19 kg/h.

How do i calculate the approximate nitrogen volume required?

Thanks in advance!

[breizh]

Hi,

Consider the document attached to support your work.

Breizh

[latexman]

Consider using API 2000, "Venting Atmospheric and. Low-Pressure Storage Tanks", or Argentina's equivalent standard.

[Quimarah]

Thank you for your answer.

Checking the API 2000  i decided to define the approximate nitrogen volume required as 42,48 Sm3/h For a 52500 gal tank of glycerol.

I don`t know if this is the right asumption.

[latexman]

Attach your calculations, assumptions, tank specs, etc and we’ll look it over.

[Art Montemayor]

Evelyn:

 

I just dropped in to see how some of my old professional friends are doing in furnishing excellent, intelligent responses to other engineers with queries.  Your thread interests me because we covered this same issue many times in the past in this forum.  The helpful responses have not changed and they are all highly recommended.

 

In order to get a detailed, accurate recommendations on how to accomplish what you want to do I highly urge you to respond to Latexman with what he is requesting.  If you do, you will obtain the kind of detailed recommendations and advice that you need to do your project safely and efficiently.  Basically, what is needed is Basic Data, the exact type and size of tank you are planning to inert, the rates of glycerin fill, the availability of the proposed inert nitrogen in flow rate, its pressure and temperature.

 

The Forum members have to have the above data and information in order to ensure that what they recommend is SAFE engineering design that will not only work, but that will carry out exactly what you require.  Some items of concern I would pass on to you are:

 

• The API 650 design has a maximlum pressure rating as well as a mazimum vacuum operation.  Be aware that when you enclose this tank with an inert gas you are subject to a potential vacuum condition as well as over-pressure.  You should hold one or several Hazops to ensure that all potential future issues and safety concerns are resolved before going forth.
• The maximum rates of glycerin inlet and outlet flows must be taken into consideration for the operation to be considered safe.
• There may be a difference between the inlet nitrogen temperature and that in the tank (50 C).  What I have done in the past is that I introduced the nitrogen through a submerged pipe in order to allow it to go through the hot (or warm) liquid fluid in order to be preheated before entering the tank's vapor space.  This stabilizes any pressure variations in the vapor space and over-feeding of nitrogen with subsequent vapor purging.
• Take careful consideration of your tank vacuum breaker and pressure relief.  I consider the vacuum breaker as a major item to design carefully.  Any sudden tank leak or major liquid outlet can cause a potential vacuum and tank collapse.
• Constant, available nitrogen supply must always be present.
• Always design for and alert all operating and maintenance personnel about the inherent dangers of nitrogen inside the tank during any mainenance or clean-out.  The nitrogen feed line should be designed with a positive method of removing a section of pipe downstream of the nitrogen feed line block valve.  Never trust that the nitrogen feed block valve is shut closed while doing internal maintenance.
• Nitrogen deaths due to asphyxiation have been far too numerous and can be halted if proper steps are taken.

 

I hope the above helps.  Saludos.

 

My best regards to all my old friends.

[latexman]

Hi Art,

Thanks for dropping in! Take care!

[breizh]

Hi Art,

Best regards from Thailand

Breizh

[hani135]

Hi,

i have a question regarding the nitrogen blanketing.

For a tank farm - receiving blanketing due to volatile organic, what is the correct method to calculate the N2 requirement? using the API 2000 7th edition :

for the pump out breathing - should i take the max flow or combine all flows? my common sense is to take the max flow (which will be of the organic multiplied by 2 - as it is volatile). in that case is will be 660 Nm3/h.

for the thermal breathing - i have some concerns.

should it be the summary of the  blanketed tanks volumes? ~3500 m3, and using table A3 from the API = 647 Nm3/h

or should i use the API equations for thermal breathing, summarize all which results in 670 Nm3/h.

 

this in total will result 660+670=1330 Nm3/h.

 

i also step upon calculation taking the head space of tanks for the thermal breathing.

 

can anyone help ?

[latexman]

Next time, do not "pile on" to an existing thread.  Make a new post/thread, please.

 

I have always applied API 2000 to individual tanks, then used the limitations of the physical facilities to determine total usages.  IMO, that is  RAGAGEP.

 

I searched my API 2000 7th Edition for the words "tank farm" and "farm" and found none.  The word "tank" is mentioned 423 times.  That may be additional proof one cannot just apply API 2000 to a summary of tank volumes for a tank farm.  What gave you the idea you could do that?  Maybe one can, and I just never have.  Anyone else have the experience?

[Pilesar]

For a similar situation, I relied on a hydraulic model of the tank farm. Each tank in the farm will have its thermal inbreathing load simultaneously since the weather affects the entire farm. Only a few tanks will have their pump-out load simultaneously. Determine the maximum reasonable number of tanks to use as design basis for pump-out and select the worst-case tanks for the pump-out list. Since hydraulics rule, it may be that the worst-case is not the one with the largest pumping rate. For example, if four tanks can pump out at the same time in the design case, the supply pressure may need to be higher if these tanks are all on the same side of the tank farm instead of distributed throughout the farm. Be aware that the nitrogen regulators at each tank will have a minimum nitrogen pressure requirement for the inlet of the regulator which is significantly higher than the storage tank design pressure. Each tank nitrogen line should have a check valve and a flow restricting orifice so a problem at one tank will not cause trouble to other tanks.

[breizh]

Hi,

If I was in your shoes, I would contact specialized companies like  Protectoseal and others.

https://www.protecto...ank-blanketing/

let you prepare a sketch to submit to them.

Breizh 

[hani135]

Thank you all.